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色譜級正庚烷的測定毛細(xì)管柱
色譜級正庚烷的測定毛細(xì)管柱 詳細(xì)信息：

名稱：毛細(xì)管柱

規(guī)格：50m*0.25mm

型號：OV-101

應(yīng)用：GB 8120-1987高純正庚烷和異辛烷純度測定法 (毛細(xì)管色譜法)

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司研發(fā)一種色譜級正庚烷的生產(chǎn)方法，涉及化工技術(shù)領(lǐng)域。該方法包括如下步驟：向工業(yè)級正庚烷中加入混酸溶液，在攪拌條件下進(jìn)行酸洗，然后靜置分層；分離出下層酸液，然后加入堿液，在攪拌條件下對正庚烷進(jìn)行堿洗，然后靜置分層；分離出下層堿液，加入純水洗滌洗滌液呈中性；然后靜置分層；分離出下層水溶液，加入干燥劑進(jìn)行干燥；然后過濾除去干燥劑；取濾液進(jìn)行蒸餾，收集98?100℃的產(chǎn)品即得。該方法通過酸洗、堿洗除去正庚烷中的雜質(zhì)，通過清水洗滌殘留的酸堿，并用干燥劑除去剩余的少量水分，蒸餾取特定溫度下的餾分得到高純度的正庚烷，該方法工藝簡單，試劑成本低廉，并且除去雜質(zhì)的同時(shí)不引入其他有機(jī)雜質(zhì)，產(chǎn)品收率高。

色譜級正庚烷的測定毛細(xì)管柱 測試譜圖：




Determination of chromatographic grade n-heptane capillary column
Capillary column for the determination of chromatographic grade n-heptane Details:

Name: Capillary Column

Specification: 50m*0.25mm

Model: OV-101

Application: GB 8120-1987 High-purity n-heptane and isooctane purity determination method (capillary chromatography)



Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. has developed a method for producing chromatographic-grade n-heptane, which involves the field of chemical technology. The method includes the following steps: adding a mixed acid solution to industrial-grade n-heptane, pickling under stirring conditions, and then standing for stratification; separating the lower layer of acid solution, then adding lye, and reacting to n-heptane under stirring conditions. Carry out alkaline washing, then stand for layering; separate the lower layer of lye, add pure water to wash until the washing liquid is neutral; then stand for layering; separate the lower layer of aqueous solution, add a desiccant to dry; then filter to remove the desiccant; Take the filtrate for distillation, and collect the product at 98-100°C. This method removes impurities in n-heptane by pickling and alkali washing, washing the remaining acid and alkali with clear water, and removing the remaining small amount of water with a desiccant, and distilling the fraction at a specific temperature to obtain high-purity n-heptane. This method The process is simple, the reagent cost is low, and other organic impurities are not introduced while removing impurities, and the product yield is high.

Determination of chromatographic grade n-heptane capillary column Test spectrum: